HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzoic acid → 4-Cyano-N-[4-(2-morpholin-4-ylethoxy)-1-naphthyl]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzoic acid | HCID 12087 | — |
| Reactant | 4-(2-Morpholinoethoxy)naphthalen-1-amine | HCID 11043912 | — |
| Product | 4-Cyano-N-[4-(2-morpholin-4-ylethoxy)-1-naphthyl]benzamide | HCID 59553360 | — |
Reaction Steps
Compound is prepared from 4-cyanobenzoic acid and 4-(2-morpholin-4-yl-ethoxy)-naphthalen-1-ylamine according to conditions described in general procedure G. Mp: 213-214° C.; 1H NMR (300 MHz, CDCl3) δ 2.70 (m, 4H), 3.00 (t, 2H), 3.78 (t, 4H), 4.35 (t, 2H), 6.80 (d, 1H), 7.50-7.70 (m, 5H), 7.80 (d, 1H), 7.95 (d, 2H), 8.31 (s, 2H); MS 402 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08114873B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-f344e0263b234f548f461274d9ee6139 |
| Source note | uspto-grants-2012_02 |