Methanol → HCID 86761491, compound

Participants

Reaction Conditions

Reaction Steps

The compound (10 g) prepared in Example 57 was dissolved in water (40 mL) and methanol (40 mL) at 53° C. To the solution, 2-propanol (1900 mL) was added and cooled to 5° C. The precipitated solid was filtered and dried at 40° C. under reduced pressure. The compound was maintained at 60% of relative humidity at 25° C. for 2 days to obtain the title compound (8.2 g) having the following physical properties.

Provenance & Evidence