Acetone → HCID 66739094, compound

Participants

Reaction Conditions

Reaction Steps

The compound (10 g) prepared in Example 58 was dissolved in water (20 mL) and methanol (20 mL) at 53° C. To the solution, acetone (750 mL) was added and cooled to 15° C. The precipitated solid was filtered and dried at 40° C. under reduced pressure. The compound was maintained at 75% of relative humidity at 40° C. for 10 days to obtain the title compound (8.2 g) having the following physical properties.

Provenance & Evidence