Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86643012 | HCID 86643012 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 86643011 | HCID 86643011 | 178.8% |
Reaction Steps
The compound (8.5 g) prepared in Example 59 was dissolved in water (22 mL) and methanol (22 mL) at 60° C. To the solution, acetone (430 mL) was added at room temperature and cooled to 2° C. The precipitated solid was filtered and dried at 50° C. under reduced pressure to obtain the title compound (7.8 g) having the following physical properties.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08115014B2 |
|---|
| Source dataset | uspto-grants-2012_02 |
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| ORD ID | ord-dc51ed7d3900496a82ee652656c70da7 |
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| Source note | uspto-grants-2012_02 |
|---|
