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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1641607Generated: November 1, 2026

Water → HCID 25026399, compound

https://huagongshe.com/reaction/1641607

Reaction equation

Participants

RoleNameHCIDCharge
ReactantWaterHCID 962—
Reactant3-(4-Hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)prop-2-en-1-oneHCID 66738878—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 25026399HCID 2502639989.3%

Reaction Steps

10 g of 3-(4-hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)-2-propen-1-one are dissolved in 100 g of tetrahydrofuran, combined with 0.2 g of Pd on activated carbon (Pd content: 5 wt. %, water content approx. 50 wt. %, in each case relative to the total mass of the catalyst) and hydrogenated at standard pressure and room temperature (approx. 20° C.) After removal of the catalyst and the solvent, 9 g of 3-(4-hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)-propan-1-one are obtained. Yield: 89% of theoretical

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08115033B2
Source datasetuspto-grants-2012_02
ORD IDord-ae5bc0505173444580c022b88680ded2
Source noteuspto-grants-2012_02