HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 25026399, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 3-(4-Hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)prop-2-en-1-one | HCID 66738878 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 25026399 | HCID 25026399 | 89.3% |
Reaction Steps
10 g of 3-(4-hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)-2-propen-1-one are dissolved in 100 g of tetrahydrofuran, combined with 0.2 g of Pd on activated carbon (Pd content: 5 wt. %, water content approx. 50 wt. %, in each case relative to the total mass of the catalyst) and hydrogenated at standard pressure and room temperature (approx. 20° C.) After removal of the catalyst and the solvent, 9 g of 3-(4-hydroxy-3-methoxyphenyl)-1-(4-hydroxyphenyl)-propan-1-one are obtained. Yield: 89% of theoretical
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08115033B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-ae5bc0505173444580c022b88680ded2 |
| Source note | uspto-grants-2012_02 |