HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66755636 | HCID 66755636 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Trifluoroacetate | HCID 84468 | — |
| Product | (3-Nitro-phenyl-N-(aminosulfonyl)amino)-acetic acid ethyl ester | HCID 66755370 | — |
Reaction Steps
5 mmol of (3-nitro-phenyl-N-(t-butylaminosulfonyl)amino)-acetic acid ethyl ester is dissolved in 20 ml of 90% aqueous TFA and the mixture obtained is stirred for 1 hour at rt. The mixture obtained is diluted with dioxane and solvent is evaporated. (3-Nitro-phenyl-N-(aminosulfonyl)amino)-acetic acid ethyl ester in the form of a trifluoroacetate is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119617B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-33cc340f28a9432b8d1dfeb5c7afd54e |
| Source note | uspto-grants-2012_02 |