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HRID1642058

反应详情

EQUATION

反应方程式

HRID 1642058 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CCOC(=O)CN(c1cccc([N+](=O)[O-])c1)S(=O)(=O)NC(C)(C)C
HCID66755636

未命名化合物

PRODUCTS

生成物

2
结构：O=C([O-])C(F)(F)F
HCID84468

Trifluoroacetate

C2F3O2-

结构：CCOC(=O)CN(c1cccc([N+](=O)[O-])c1)S(N)(=O)=O
HCID66755370

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1COCCO1
溶剂HCID31275

1,4-Dioxane

C4H8O2

PROCEDURE

实验过程

5 mmol of (3-nitro-phenyl-N-(t-butylaminosulfonyl)amino)-acetic acid ethyl ester is dissolved in 20 ml of 90% aqueous TFA and the mixture obtained is stirred for 1 hour at rt. The mixture obtained is diluted with dioxane and solvent is evaporated. (3-Nitro-phenyl-N-(aminosulfonyl)amino)-acetic acid ethyl ester in the form of a trifluoroacetate is obtained.

WORKUP

后处理

  1. customthe mixture obtained
  2. customThe mixture obtained
  3. customis evaporated