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HRID1642060

反应详情

EQUATION

反应方程式

HRID 1642060 的结构方程式

REACTANTS

反应物

3
结构：Cc1ccccc1
HCID1140

Toluene

C7H8

结构：CCOP(OCC)OCC
HCID31215

Triethyl phosphite

C6H15O3P

结构：O=[N+]([O-])C(Br)c1ccccc1
HCID11356361

nitrobenzylbromide

C7H6BrNO2

PRODUCTS

生成物

1
结构：CCOP(=O)(Cc1ccccc1[N+](=O)[O-])OCC
HCID11277310

Diethyl 2-nitrobenzylphosphonate

C11H16NO5P

PROCEDURE

实验过程

A mixture of 1.02 g of nitrobenzylbromide and 1.08 ml of triethylphosphite in 10 ml of toluene is heated to reflux for 12 hours. From the mixture obtained solvent is evaporated. (2-Nitro-benzyl)-phosphonic acid diethyl ester is obtained.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureto reflux for 12 hours
  3. customFrom the mixture obtained solvent
  4. customis evaporated