HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → Diethyl 2-nitrobenzylphosphonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triethyl phosphite | HCID 31215 | — |
| Reactant | Nitrobenzylbromide | HCID 11356361 | — |
| Product | Diethyl 2-nitrobenzylphosphonate | HCID 11277310 | — |
Reaction Steps
A mixture of 1.02 g of nitrobenzylbromide and 1.08 ml of triethylphosphite in 10 ml of toluene is heated to reflux for 12 hours. From the mixture obtained solvent is evaporated. (2-Nitro-benzyl)-phosphonic acid diethyl ester is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119617B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-8020bf7922cc4cde921b1f2d294bf530 |
| Source note | uspto-grants-2012_02 |