HRID1642061

反应详情

EQUATION

反应方程式

HRID 1642061 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

1.13 g of (2-nitro-benzyl)-phosphonic acid diethyl ester) in ethanol are hydrogenated with Pd—C as a catalyst for 5 hours at rt and ambient pressure. The catalyst is removed by filtration and from the filtrate obtained solvent is evaporated. (2-Amino-benzyl)-phosphonic acid diethyl ester is obtained.

WORKUP

后处理

  1. customThe catalyst is removed by filtration and from the filtrate
  2. customobtained solvent
  3. customis evaporated