HCID 57619803, compound → HCID 57619825, compound

Participants

Reaction Steps

A solution of tert-butyl 4-[4-[(3aR,7aS)-2-oxo-3a,4,5,6,7,7a-hexahydro-3H-indol-1-yl]-1-piperidyl]-4-methyl-piperidine-1-carboxylate in MeOH (14 mL) and 4M HCl in dioxane (5 mL) was stirred at room temperature overnight. Concentrated in vacuo and the residue was purified by preparative LC/MS (high pH) to provide the title compound as a colorless oil (0.41 g). MS (M+1): 320.30.

Provenance & Evidence