HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 55288821, compound → HCID 57619819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 55288821 | HCID 55288821 | — |
| Reactant | HCID 57619795 | HCID 57619795 | — |
| Product | HCID 57619819 | HCID 57619819 | 9% |
Reaction Steps
Following the procedure used in step D of the example 14 and starting with 2-[(1R,2S)-2-aminocyclohexyl]acetonitrile (0.342 g, 2.47 mmol) and tert-butyl 3-methyl-3-(4-oxo-1-piperidyl)pyrrolidine-1-carboxylate (0.699 g, 2.47 mmol), the title compound (0.090 g, 8.99%) was obtained after purification by preparative LC/MS (High pH). MS (M+1): 405.23.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119661B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-9ec1a8d5b5e94626bf078718896b02c6 |
| Source note | uspto-grants-2012_02 |