反应详情

The title compound was synthesized from Compound 157 using an analogous procedure to that outlined in the preparation of Compound 205. 1H NMR (400 MHz, MeOD) δ ppm 1.29 (t, J=7.33 Hz, 3 H) 2.32 (s, 3 H) 2.91 (t, J=5.31 Hz, 2 H) 4.34 (t, J=5.43 Hz, 2H) 7.07-7.14 (m, 2 H) 7.65 (d, J=2.02 Hz, 1 H) 7.82 (t, J=7.83 Hz, 1 H) 7.94-7.98 (m, 1 H) 8.02 (dd, J=7.33, 1.52 Hz, 1 H) 8.15 (t, J=1.64 Hz, 1 H) 8.20 (d, J=2.02 Hz, 1 H) [M+H] calc'd for C24H27N3O3S, 438; found, 438.