HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol → HCID 58880171, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-ol | HCID 58880081 | — |
| Reactant | 3-(5-(3-(ethylsulfonyl)phenyl)-3-methyl-9H-pyrido[2,3-b]indol-8-yloxy)-N,N-dimethylpropan-1-amine | HCID 58880181 | — |
| Product | HCID 58880171 | HCID 58880171 | — |
Reaction Steps
The title compound was synthesized from Compound 157 using an analogous procedure to that outlined in the preparation of Compound 205. 1H NMR (400 MHz, MeOD) δ ppm 1.29 (t, J=7.33 Hz, 3 H) 2.32 (s, 3 H) 2.91 (t, J=5.31 Hz, 2 H) 4.34 (t, J=5.43 Hz, 2H) 7.07-7.14 (m, 2 H) 7.65 (d, J=2.02 Hz, 1 H) 7.82 (t, J=7.83 Hz, 1 H) 7.94-7.98 (m, 1 H) 8.02 (dd, J=7.33, 1.52 Hz, 1 H) 8.15 (t, J=1.64 Hz, 1 H) 8.20 (d, J=2.02 Hz, 1 H) [M+H] calc'd for C24H27N3O3S, 438; found, 438.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119655B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-a1aac147e0984a57b7d3008cd4047233 |
| Source note | uspto-grants-2012_02 |