HRID1642576

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CCS(=O)(=O)c1cccc(-c2ccc(OCCO)c3[nH]c4ncc(C)cc4c23)c1

HCID58880169

未命名化合物

结构：CCS(=O)(=O)c1cccc(-c2ccc(O)c3[nH]c4ncc(Cl)cc4c23)c1

HCID58880180

未命名化合物

PRODUCTS

生成物

结构：CCS(=O)(=O)c1cccc(-c2ccc(OCCO)c3[nH]c4ncc(Cl)cc4c23)c1

HCID58880090

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from Compound 218 by using an analogous procedure to that outlined in the preparation of Compound 215. 1H NMR (400 MHz, Methanol-d4) δ 8.39 (s, 1 H) 8.14 (m, 1 H) 8.06 (m, 1 H) 8.00 (m, 1 H) 7.87 (t, J=8.0 Hz, 1 H) 7.71 (d, J=4.0 Hz, 1 H) 7.21 (d, J=8.0 Hz, 1 H) 7.16 (d, J=8.0 Hz, 1 H) 4.36 (t, J=4 Hz, 2 H) 4.07 (t, J=4 Hz, 2 H) 3.30 (q, J=7.5 Hz, 2 H) 1.31 (t, J=7.5 Hz, 3 H). [M+H] calc'd for C21H20ClN2O4S, 431; found, 431.