HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine-2-carbonitrile → N-Hydroxypicolinimidamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine-2-carbonitrile | HCID 7522 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hydroxylamine HCl | HCID 21645 | — |
| Product | N-Hydroxypicolinimidamide | HCID 120564 | — |
Reaction Steps
1.0 g (9.6 mmol) of pyridine-2-carbonitrile, 1.0 g (14.4 mmol) of hydroxylammonium chloride and 1.6 ml (11.5 mmol) of triethylamine were reacted according to the General Method 5A. Yield: 1.06 g (80% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-f471a93519bf463e942001a87fdadda8 |
| Source note | uspto-grants-2012_02 |