HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 57374593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Hydroxylamine HCl | HCID 21645 | — |
| Reactant | 4-Methyl-3-cyanopyridine | HCID 227806 | — |
| Product | HCID 57374593 | HCID 57374593 | — |
Reaction Steps
850 mg (7.20 mmol) of 4-methylpyridine-3-carbonitrile, 750 mg (10.79 mmol) of hydroxylammonium chloride and 1.2 ml (8.6 mmol) of triethylamine were reacted according to the General Method 5A. Yield: 666 mg (61% of theory)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-0971bb7babbf45ed8c3e87555cbdd073 |
| Source note | uspto-grants-2012_02 |