HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1-Dichloroacetone → HCID 58002246, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1-Dichloroacetone | HCID 10567 | — |
| Reactant | HCID 58002396 | HCID 58002396 | — |
| Product | HCID 58002246 | HCID 58002246 | — |
Reaction Steps
860 mg (2.38 mmol) of 5-(4-ethylphenyl)-1-(morpholin-4-ylcarbonyl)piperidine-3-carbothioamide (Example 140A) and 362 mg (2.85 mmol) of dichloroacetone were reacted according to the General Method 3. Yield: 498 mg (43% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-9f60253d9d8840829fa11983280e3340 |
| Source note | uspto-grants-2012_02 |