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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1642975Generated: November 1, 2026

Hydrochloric Acid → HCID 66755065, compound

https://huagongshe.com/reaction/1642975

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 58002498HCID 58002498—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66755065HCID 66755065—

Reaction Steps

0.12 ml (0.50 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 29 mg (about 0.05 mmol) of the compound from Example 86A in 0.2 ml of dioxane. The reaction mixture was stirred at room temperature for 20 hours. The mixture was then concentrated to dryness under reduced pressure and dried until the weight remained constant. Yield: 24 mg (96% of theory).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08119663B2
Source datasetuspto-grants-2012_02
ORD IDord-dc98869aad1d40e1bf6ec8e142177480
Source noteuspto-grants-2012_02