HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66755065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58002498 | HCID 58002498 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66755065 | HCID 66755065 | — |
Reaction Steps
0.12 ml (0.50 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 29 mg (about 0.05 mmol) of the compound from Example 86A in 0.2 ml of dioxane. The reaction mixture was stirred at room temperature for 20 hours. The mixture was then concentrated to dryness under reduced pressure and dried until the weight remained constant. Yield: 24 mg (96% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-dc98869aad1d40e1bf6ec8e142177480 |
| Source note | uspto-grants-2012_02 |