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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1642976Generated: October 31, 2026

Hydrochloric Acid → HCID 66755645, compound

https://huagongshe.com/reaction/1642976

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 58002140HCID 58002140—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66755645HCID 66755645—

Reaction Steps

0.11 ml (0.45 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 25 mg (0.05 mmol) of the compound from Example 88A in 0.2 ml of dioxane. The reaction mixture was stirred at room temperature for 20 hours. The mixture was then concentrated to dryness under reduced pressure and dried until the weight remained constant. Yield: 20 mg (93% of theory).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08119663B2
Source datasetuspto-grants-2012_02
ORD IDord-a403baab6b174cc28b2684e04ad4d8ce
Source noteuspto-grants-2012_02