HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66755803, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58002720 | HCID 58002720 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66755803 | HCID 66755803 | — |
Reaction Steps
0.43 ml (1.73 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 96 mg (0.17 mmol) of the compound from Example 90A in 0.8 ml of dioxane, and the mixture was stirred at room temperature for 24 h. The reaction mixture was then concentrated under reduced pressure, dichloromethane was added and the mixture was concentrated again. Yield: 85 mg (99% of theory).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119663B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-41aaec2314ba4ecdb0d038e6b1398ad0 |
| Source note | uspto-grants-2012_02 |