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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1643091Generated: October 31, 2026

Hydrochloric Acid → HCID 66755803, compound

https://huagongshe.com/reaction/1643091

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 58002720HCID 58002720—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66755803HCID 66755803—

Reaction Steps

0.43 ml (1.73 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 96 mg (0.17 mmol) of the compound from Example 90A in 0.8 ml of dioxane, and the mixture was stirred at room temperature for 24 h. The reaction mixture was then concentrated under reduced pressure, dichloromethane was added and the mixture was concentrated again. Yield: 85 mg (99% of theory).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08119663B2
Source datasetuspto-grants-2012_02
ORD IDord-41aaec2314ba4ecdb0d038e6b1398ad0
Source noteuspto-grants-2012_02