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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1643121Generated: November 1, 2026

Hydrochloric Acid → HCID 66755328, compound

https://huagongshe.com/reaction/1643121

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 58002128HCID 58002128—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 66755328HCID 66755328—

Reaction Steps

0.36 ml (1.46 mmol) of a 4N solution of hydrogen chloride in dioxane was added to a solution of 84 mg (0.146 mmol) of the compound from Example 91A in 0.7 ml of dioxane, and the mixture was stirred at room temperature for 20 hours. The reaction mixture was then concentrated under reduced pressure, dichloromethane was added and the mixture was concentrated again. Yield: 74 mg (98% of theory).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08119663B2
Source datasetuspto-grants-2012_02
ORD IDord-4317e9b9fad640e8b7de7a43d7ba656f
Source noteuspto-grants-2012_02