HRID1643127

反应详情

EQUATION

反应方程式

HRID 1643127 的结构方程式

PROCEDURE

实验过程

100 mg (0.249 mmol) of the compound from Example 44A and 32 mg (0.273 mmol) of 3-methylbutanehydrazide were reacted according to the General Method 4. Diastereomer separation of the cis/trans isomer mixture according to Method 14C gave 44 mg of the title compound (cis isomer) and 12 mg of the trans isomer.

WORKUP

后处理

  1. customDiastereomer separation of the cis/trans isomer mixture