HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 77174849, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2,4-Bis(benzyloxy)-5-bromobenzoic acid | HCID 46915638 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Product | HCID 77174849 | HCID 77174849 | — |
Reaction Steps
1.4 9 g of 5-bromo-2,4-dibenzyloxybenzoic acid, 40 ml of thionyl chloride and 1 drop of DMF are stirred at room temperature for 4 hours. The thionyl chloride is removed, and the residue is treated twice with dichloromethane, giving 9.4 g of 5-bromo-2,4-dibenzyloxybenzoyl chloride, which is processed further directly.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119795B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-0ed69b3e5b3c4b8fb8345c2ebf4e322d |
| Source note | uspto-grants-2012_02 |