HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 178424333, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 178418416 | HCID 178418416 | — |
| Reactant | HCID 178424332 | HCID 178424332 | — |
| Catalyst | Bis(cyclopenta-1,4-dien-1-yl(diphenyl)phosphane);dichloropalladium;iron(2+) | HCID 178418228 | — |
| Product | HCID 178424333 | HCID 178424333 | — |
Reaction Steps
7.3 g of 5-(2,4-dibenzyloxy-5-bromophenyl)-4-(2-methylphenyl)-3-hydroxy-4H-1,2,4-triazole, 150 ml of methanol, 0.3 l of carbon monoxide, 150 mg of [1,1′-bis(diphenylphosphino)ferrocene]dichloropalladium(II), 2 g of triethylamine and 10 ml of toluene.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119795B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-febdc58c96804ae0825e53f1c5691181 |
| Source note | uspto-grants-2012_02 |