HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59367762, compound → HCID 57819729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59367762 | HCID 59367762 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57819729 | HCID 57819729 | — |
Reaction Steps
A degassed solution of (E)-ethyl 3-(1-(4-methoxy-2,6-dimethylphenylsulfonyl)-piperidin-2-yl)acrylate (4.19 mmol) in MeOH was hydrogenolysed with Pd(OH)2 (0.4 g) as the catalyst. The resulting crude product was employed in the following stage without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08119805B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-b705a966210f4f2b83c8fd4932187d8e |
| Source note | uspto-grants-2012_02 |