HuagongsheHuagongshe Chemistry Print Report · For research reference only
Titanium isopropoxide → HCID 86597431, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Titanium isopropoxide | HCID 11026 | — |
| Reactant | Acetylacetone | HCID 31261 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86597431 | HCID 86597431 | — |
Reaction Steps
To a dried vial fitted with a stir bar and septum cap was added titanium tetraisopropoxide (2.8573 g, 1.005 mmol) then 2,4-pentanedione (1.0257 g, 1.0245 mmol), and quickly cooled in an ice water bath. The dark yellow liquid was stirred overnight at room temperature. The solution was then diluted with 32.4 ml ethanol (200 proof).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124443B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-af15b81d7ba64693bb5e2cc375777a8c |
| Source note | uspto-grants-2012_02 |