Titanium isopropoxide → HCID 86597431, compound

HRID 1644161Notes

Reaction equation

HRID 1644161 reaction equation
CC(C)[O-].CC(C)[O-].CC(C)[O-].CC(C)[O-].[Ti+4:17].[CH3:18][C:19](=[O:24])[CH2:20][C:21](=[O:23])[CH3:22]>C(O)C>[C:21]([CH2:20][C:19](=[O:24])[CH3:18])(=[O:23])[CH3:22].[C:21]([CH2:20][C:19](=[O:24])[CH3:18])(=[O:23])[CH3:22].[Ti:17]

Participants

4

Reactant 2

HCID 11026Titanium isopropoxideHCID 31261Acetylacetone

Product 1

HCID 86597431HCID 86597431, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To a dried vial fitted with a stir bar and septum cap was added titanium tetraisopropoxide (2.8573 g, 1.005 mmol) then 2,4-pentanedione (1.0257 g, 1.0245 mmol), and quickly cooled in an ice water bath. The dark yellow liquid was stirred overnight at room temperature. The solution was then diluted with 32.4 ml ethanol (200 proof).

Workup

  1. customTo a dried vial fitted with a stir bar
  2. customseptum cap

Sources & evidence

ORD record
ord-af15b81d7ba64693bb5e2cc375777a8c
Source dataset
uspto-grants-2012_02
Patent number
US08124443B2

Reaction notes

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