HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoylhydrazine → N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoylhydrazine | HCID 11955 | — |
| Reactant | Cinnamaldehyde | HCID 637511 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | N-[(E)-[(E)-3-phenylprop-2-enylidene]amino]benzamide | HCID 6870846 | 90% |
Reaction Steps
A mixture of 1a (3.00 g, 22.0 mmol) and trans cinnamic aldehyde (4.35 g, 32.9 mmol, origin: Aldrich) in hexane (100 ml) was stirred at room temperature for 2 h. The reaction mixture was filtered, the residue washed with hexane and dried under vacuum to give 4.95 g (90%) of a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124578B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-68e97b156d944ea29316e7a2c7a8d981 |
| Source note | uspto-grants-2012_02 |