反应详情

A mixture of 1a (1.50 g, 11.0 mmol) and 10-undecenal (2.80 g, 16.5 mmol) in ethanol (28 ml) was heated under reflux for 2 h. After cooling to room temperature, the product was concentrated, washed with hexane and dried under vacuum (0.20 mbar) to give 2.78 g (88%) of a white solid.

1. temperaturewas heated
2. temperatureunder reflux for 2 h
3. concentrationthe product was concentrated
4. washwashed with hexane
5. customdried under vacuum (0.20 mbar)