HRID1644304

反应详情

EQUATION

反应方程式

HRID 1644304 的结构方程式

PROCEDURE

实验过程

The compound was prepared from 3-fluoroaniline (5.8 mL, 60 mmol) and cinnamoylchloride (10 g, 60 mmol) in the presence of 2,6-lutidine (10.5 mL, 90 mmol) as described for Intermediate 18 to give a colorless solid, 13.9 g (96%), mp 110° C.

WORKUP

后处理

  1. customto give a colorless solid, 13.9 g (96%), mp 110° C.