HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 178458532, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 178458530 | HCID 178458530 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178458532 | HCID 178458532 | — |
Reaction Steps
A solution (10 ml) of 2-[5-(benzyloxy)-2-isopropoxyphenyl]-3H-imidazo[4,5-b]pyridine (0.2 g) and m-chloroperbenzoic acid (0.15 g) in chloroform was stirred at room temperature for 18 hr. The reaction mixture was washed with aqueous sodium hydrogencarbonate solution, dried over magnesium sulfate and concentrated to give the title compound as colorless crystals. purity 80%. M+H: 376.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124617B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-aa724118d7ce49c9958965d8bf093f64 |
| Source note | uspto-grants-2012_02 |