HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 4065164, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 3-Amino-5-nitrobenzoic acid | HCID 239342 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 4065164 | HCID 4065164 | — |
Reaction Steps
3-Amino-5-nitrobenzoic acid ([23218-93-1], 0.99 g, 5.05 mmol) was stirred in DCM (20 mL) and pyridine (2 mL) at 0° C. Acetic anhydride (1 mL, 10 mmol) was added. The reaction was stirred overnight. Water (30 mL) was added. A precipitate formed and was collected by filtration. [M+H] calc'd for C10H10N2O5 239; found, 239.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124617B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-b2e16b753bfc4af88dd9dbe2e38f76cb |
| Source note | uspto-grants-2012_02 |