HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 59243016, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58948855 | HCID 58948855 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59243016 | HCID 59243016 | — |
Reaction Steps
Methyl 3-(2-fluorobenzyloxy)-5-hydroxybenzoate (224a), 10 mL of Methyl alcohol and 10 mL of 1N NaOH were stirred at ambient temperature for 4 h, acidified with 1N HCl until neutral and extracted into ethyl acetate. The combined organic extracts were dried over magnesium sulfate, filtered and evaporated. The LC/MS gave a calculated and found (M+H+)=263.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124617B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-1cdaf8256b274c8c83e169adb3015e5e |
| Source note | uspto-grants-2012_02 |