HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 66773538, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 66773211 | HCID 66773211 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 66773538 | HCID 66773538 | — |
Reaction Steps
This material was prepared in analogy to example 1 and 2, step A, using 2-benzyloxymethyl-pyrrolidine-1,2-dicarboxylic acid 1-tert-butyl ester (1.426 g, see example 12, step A) and ammonia solution (320 μL of a 25% solution in water) to give the desired (rac)-2-benzyloxymethyl-2-carbamoyl-pyrrolidine-1-carboxylic acid tert-butyl ester (1.5 g, MS (ES+): 335.3 (MH+)) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124636B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-4572ff55a7e647aa8e6734884472c2ca |
| Source note | uspto-grants-2012_02 |