HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 11716370, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | 5,6-Dimethoxy-2-(pyridin-4-ylmethyl)indan-1-one | HCID 10085230 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 11716370 | HCID 11716370 | — |
Reaction Steps
4-[(5,6-Dimethoxy-1-indanon-2-yl)methyl]pyridine (1.2 g) was dissolved in methylene chloride (18 ml) and chilled. m-Chloroperbenzoic acid (0.9 g) was added to reaction mixture and then stirred for 4 hours. Reaction mass was stirred with 10% aqueous solution of sodium bicarbonate. The organic layer was separated and washed with 50 ml water. Organic layer was distilled off, title compound is obtained (1.2 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124783B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-19c517e487684d399488a8cb32151c3d |
| Source note | uspto-grants-2012_02 |