Hydrochloric Acid → HCID 372723, compound

Participants

Reaction Steps

A solution of 1.25 g of KMnO4 and 7.8 mL of conc. HCl in 115 mL of ice cooled H2O was stirred for 2 hrs. To this solution was added 2.02 g of ethylene methanedisulfonate in 25 mL of 0.5 molar NaOH. The solid obtained after acidification was placed in 15 mL of 0.5 M NaOH and the filtrate acidified to give 1.1 g of ethylene chloromethanedisulfonate, m.p. 85-88° C. (91-6).

Provenance & Evidence