Hydrochloric Acid → HCID 372723, compound

HRID 1645406Notes

Reaction equation

HRID 1645406 reaction equation
[O-][Mn](=O)(=O)=O.[K+].[ClH:7].O.[CH2:9]1[S:17](=[O:19])(=[O:18])[O:16][CH2:15][CH2:14][O:13][S:10]1(=[O:12])=[O:11]>[OH-].[Na+]>[Cl:7][CH:9]1[S:10](=[O:11])(=[O:12])[O:13][CH2:14][CH2:15][O:16][S:17]1(=[O:19])=[O:18]

Participants

6

Reactant 4

HCID 313Hydrochloric AcidHCID 962WaterHCID 57513CyclodisoneHCID 516875Potassium Permanganate

Product 1

HCID 372723HCID 372723, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent2×

Procedure

A solution of 1.25 g of KMnO4 and 7.8 mL of conc. HCl in 115 mL of ice cooled H2O was stirred for 2 hrs. To this solution was added 2.02 g of ethylene methanedisulfonate in 25 mL of 0.5 molar NaOH. The solid obtained after acidification was placed in 15 mL of 0.5 M NaOH and the filtrate acidified to give 1.1 g of ethylene chloromethanedisulfonate, m.p. 85-88° C. (91-6).

Workup

  1. customThe solid obtained after acidification

Sources & evidence

ORD record
ord-22d6ed5cbbcf46878231f07a8ee090bb
Source dataset
uspto-grants-2012_02
Patent number
US08124793B2

Reaction notes

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