HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → HCID 86632336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Cyclodisone | HCID 57513 | — |
| Solvent | 1,2-Dimethoxyethane | HCID 8071 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 86632336 | HCID 86632336 | 34.7% |
Reaction Steps
To a solution of 2.6 g of ethylene methanedisulfonate in 50 mL of glyme and 1.0 g of NaH was added 3 g of benzyl chloride. After rotoevaporation of the glyme the residue was taken up in 25 mL of 0.5 M NaOH, filtered, and acidified to give 1.21 g of ethylene benzyl methanedisulfonate, m.p. 170-174° C. (90-3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124793B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-0eedd579fd3946a8ac960fffda874f49 |
| Source note | uspto-grants-2012_02 |