Thionyl Chloride → HCID 18429135, compound

HRID 1645494Notes

Reaction equation

HRID 1645494 reaction equation
[C:1]([O:4][CH:5]([CH:9]([O:15][C:16](=[O:18])[CH3:17])[CH2:10][O:11][C:12](=[O:14])[CH3:13])[C:6](O)=[O:7])(=[O:3])[CH3:2].S(Cl)([Cl:21])=O>>[C:16]([O:15][CH:9]([CH:5]([O:4][C:1](=[O:3])[CH3:2])[C:6]([Cl:21])=[O:7])[CH2:10][O:11][C:12](=[O:14])[CH3:13])(=[O:18])[CH3:17]

Participants

3

Reactant 2

HCID 24386Thionyl ChlorideHCID 77215762HCID 77215762, compound

Product 1

HCID 18429135HCID 18429135, compound

Procedure

The 2,3,4-triacetoxy-butyric acid (25 g, 0.095 mol) was stirred in thionyl chloride (15.3 mL) at room temperature with a condenser fitted. The reaction was stirred for 48 hours and then the thionyl chloride was removed under reduced pressure to give an oil which was the desire material (26.1 g, 98%).

Workup

  1. customfitted
  2. customthe thionyl chloride was removed under reduced pressure
  3. customto give an oil which

Sources & evidence

ORD record
ord-0046802a94544cd6b00d157b03fbf1bc
Source dataset
uspto-grants-2012_02
Patent number
US08124806B2

Reaction notes

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