HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 18429135, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 77215762 | HCID 77215762 | — |
| Product | HCID 18429135 | HCID 18429135 | — |
Reaction Steps
The 2,3,4-triacetoxy-butyric acid (25 g, 0.095 mol) was stirred in thionyl chloride (15.3 mL) at room temperature with a condenser fitted. The reaction was stirred for 48 hours and then the thionyl chloride was removed under reduced pressure to give an oil which was the desire material (26.1 g, 98%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124806B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-0046802a94544cd6b00d157b03fbf1bc |
| Source note | uspto-grants-2012_02 |