HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl ketone → (2,2-Diethyl-1,3-dioxan-5-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl ketone | HCID 7288 | — |
| Reactant | Trimethylolmethane | HCID 78432 | — |
| Product | (2,2-Diethyl-1,3-dioxan-5-yl)methanol | HCID 14629254 | 46% |
Reaction Steps
The same procedure as in the step (7a) of Example 7 was repeated using 2-(hydroxymethyl)-1,3-propanediol, and 3-pentanone to obtain the title compound (1.5 g, yield: 46%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-295a813ba4fb4d6fb0367b372dcc9cde |
| Source note | uspto-grants-2012_02 |