HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetoacetate → 2-(6-Methyl-5,7-dioxaspiro[2.5]oct-6-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetoacetate | HCID 8868 | — |
| Reactant | 2-(2-Propyl-1,3-dioxan-2-yl)ethanol | HCID 59792435 | — |
| Product | 2-(6-Methyl-5,7-dioxaspiro[2.5]oct-6-yl)ethanol | HCID 59792495 | 36% |
Reaction Steps
The same procedure as in the steps (8a) and (8b) of Example 8, was repeated using ethyl acetoacetate and 1,1-bis(hydroxymethylcyclopropane) to obtain the title compound (2.9 g, total yield: 36%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-993da1d13e5b4d82bcd4cb935eb86ead |
| Source note | uspto-grants-2012_02 |