HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methoxyacetoacetate → 2-(2-(Methoxymethyl)-1,3-dioxan-2-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methoxyacetoacetate | HCID 123500 | — |
| Reactant | 2-(2-Propyl-1,3-dioxan-2-yl)ethanol | HCID 59792435 | — |
| Product | 2-(2-(Methoxymethyl)-1,3-dioxan-2-yl)ethanol | HCID 59792549 | 34% |
Reaction Steps
The same procedure as in the steps (8a) and (8b) of Example 8 was repeated using methyl 4-methoxyacetoacetate to obtain the title compound (4.5 g, total yield: 34%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-7913e323612a44639fa31b3d52f20879 |
| Source note | uspto-grants-2012_02 |