HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanocyclobutane → (1-Cyclobutyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanocyclobutane | HCID 78148 | — |
| Reactant | (1-Cyclopropyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol | HCID 59792605 | — |
| Product | (1-Cyclobutyl-2,6,7-trioxabicyclo[2.2.2]oct-4-yl)methanol | HCID 59792382 | 51% |
Reaction Steps
The same procedure as in the steps (37a) to (37c) of Example 37 was repeated using cyclobutanecarbonitrile to obtain the title compound (15 g, total yield: 51%) as a light yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-0a6c2d11c0714f15af0abe829eaa77a1 |
| Source note | uspto-grants-2012_02 |