HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-methoxyacetoacetate → 2-(2-(Methoxymethyl)-1,3-dioxolan-2-yl)ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-methoxyacetoacetate | HCID 123500 | — |
| Reactant | 2-(2-Ethyl-1,3-dioxolan-2-yl)ethan-1-ol | HCID 13940368 | — |
| Product | 2-(2-(Methoxymethyl)-1,3-dioxolan-2-yl)ethanol | HCID 59792568 | 50% |
Reaction Steps
The same procedure as in the step (39a) and (39b) of Example 39 was repeated using methyl 4-methoxyacetoacetate to obtain the title compound (5.3 g, 2 steps: 50%) as a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-5e0c73bb359d4ff3a6380d2798e51d99 |
| Source note | uspto-grants-2012_02 |