HuagongsheHuagongshe Chemistry Print Report · For research reference only
5,5-Dimethyl-1,3-dioxane-2-ethanol → 2-(((4-(2-(5,5-Dimethyl-1,3-dioxan-2-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5,5-Dimethyl-1,3-dioxane-2-ethanol | HCID 4192179 | — |
| Reactant | 2-(((4-((5,5-Dimethyl-1,3-dioxan-2-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776588 | — |
| Product | 2-(((4-(2-(5,5-Dimethyl-1,3-dioxan-2-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt | HCID 66776217 | — |
Reaction Steps
The same procedure as in the steps (1c) to (1g) of Example 1 was repeated using 5,5-dimethyl-1,3-dioxane-2-ethanol (1.00 g, 6.24 mmol) to obtain the title compound (138 mg, 0.31 mmol) as a beige solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08124780B2 |
| Source dataset | uspto-grants-2012_02 |
| ORD ID | ord-7791fc01ff2f48a486fcef2eeae50c9c |
| Source note | uspto-grants-2012_02 |