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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1645657Generated: October 30, 2026

5,5-Dimethyl-1,3-dioxane-2-ethanol → 2-(((4-(2-(5,5-Dimethyl-1,3-dioxan-2-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium salt

https://huagongshe.com/reaction/1645657

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5,5-Dimethyl-1,3-dioxane-2-ethanolHCID 4192179—
Reactant2-(((4-((5,5-Dimethyl-1,3-dioxan-2-yl)methoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium saltHCID 66776588—
Product2-(((4-(2-(5,5-Dimethyl-1,3-dioxan-2-yl)ethoxy)-3-methylpyridin-2-yl)methyl)sulfinyl)-1h-benzimidazole sodium saltHCID 66776217—

Reaction Steps

The same procedure as in the steps (1c) to (1g) of Example 1 was repeated using 5,5-dimethyl-1,3-dioxane-2-ethanol (1.00 g, 6.24 mmol) to obtain the title compound (138 mg, 0.31 mmol) as a beige solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08124780B2
Source datasetuspto-grants-2012_02
ORD IDord-7791fc01ff2f48a486fcef2eeae50c9c
Source noteuspto-grants-2012_02