HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 18369502, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 19802545 | HCID 19802545 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18369502 | HCID 18369502 | 64% |
Reaction Steps
To 0.37 g (1.48 mmol) of 2-acetyl-3-methoxy-N,N-diethylbenzamide* in 5 ml of water was added 5 ml of anhydrous hydrazine. This was heated at reflux for four hours, cooled and the resulting solid filtered and washed with water to provide 0.18 g (64%) of the desired product; mp 257°-260°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177075 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-adfd26f1ec99423b8fdad216330f23d1 |
| Source note | uspto-grants-1993_01 |