HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-benzyl-L-alanine → HCID 19100956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-benzyl-L-alanine | HCID 723764 | — |
| Reactant | Ethyl allyl(2-oxoethyl)carbamate | HCID 11084330 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 19100956 | HCID 19100956 | — |
Reaction Steps
42.8 g (0.25 mol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 44.8 g (0.25 mol) of N-benzylalanine in 750 ml of toluene. The mixture is concentrated and the residue is distilled twice.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05177210 |
| Source dataset | uspto-grants-1993_01 |
| ORD ID | ord-0c7ffcf2948a4152814a08a8c4258807 |
| Source note | uspto-grants-1993_01 |