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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1646008Generated: October 31, 2026

Pipecolic Acid → HCID 54122708, compound

https://huagongshe.com/reaction/1646008

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPipecolic AcidHCID 849—
ReactantEthyl allyl(2-oxoethyl)carbamateHCID 11084330—
SolventTolueneHCID 1140—
ProductHCID 54122708HCID 54122708—

Reaction Steps

17.1 g (0.1 mol) of ethyl N-allyl-N-(2-oxoethyl)-carbamate are heated under reflux overnight with 13 g (0.1 mol) of piperidine-2-carboxylic acid in 200 ml of toluene. The mixture is concentrated and the residue is distilled.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05177210
Source datasetuspto-grants-1993_01
ORD IDord-6f6dc2b50fac43c6bdaaa678b51c4995
Source noteuspto-grants-1993_01